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TDS

Introduction

TDS stands for Thermal Desorption Spectroscopy, a device used to measure and analyze gases desorbed from the surface of a sample as its temperature is increased. 

This method provides precise information about the binding energy of each molecule. 

Utilizing this technology enables the detection of changes in the quantity and composition of gases to trace amounts in ultra-high vacuum conditions, allowing for both qualitative and quantitative measurement of changes over time and temperature. 

Among analytical techniques, TDS is notable for its high sensitivity and stability without the need for chemicals.

What is TDS?

TDS is a device used to measure and analyze gases that are desorbed from the surface of a sample as its temperature is increased. 

It is employed to perform qualitative and quantitative analyses of gases emitted during processes, allowing for the early detection and prevention of issues by analyzing their causes.


 

Why TDS?

Simple Idea : Adsorbed particles with different binding energies will desorb at different temperature. 


 

Applications

  • - Semiconductor and Display Material Analysis
  • - Hydrogen Analysis in Automotive and Steel Materials
  • - Ultra-Pure Material and Trace Analysis

The technique of examining impurities (outgassing rate) based on temperature elevation typically employs the TDS method. However, to date, there has not been a well-established method for local and directional real-time impurity mapping on wafers, and systems capable of conducting both qualitative and quantitative analyses simultaneously are virtually non-existent. Our company provides a TDS system that overcomes these limitations.


 

Performance Comparisions

IVT's TDS system boasts competitive advantages such as calibration, heating, and pumping speed over those of other companies. 

Additionally, depending on the application area, we offer user-friendly DAQ (Data Acquisition) software. 

fTDS(Fusion)&TVGAIVT sTDS(smal)mTDS(moduated)Company ACompany BtTDS(throughput)
Measurement MethodThroughtput⑴
mapping capability
Throughtput⑴Modulation⑴QMS signal⑵QMS signal⑵Throughtput⑴
CalibrationO: direct KRISS
measurement
traceability
O: direct KRISS
measurement
traceability
O: direct KRISS
measurement
traceability
Δ indirect
traceability,
standard sample
required
Δ indirect
traceability,
standard sample
required
O: direct NMI
measurement
traceability
Sample300mm wafer, Ø60mmØ20mm SampleØ20mm SampleØ10mm SampleØ10mm SampleØ10mm Sample
HeaterBeam heater
Lamp heater
IR rod heaterIR rod heaterIR rod heaterFurnace : PID DifficultIR rod heater
Hydrogen Pumping
Speedr
Method 1 : not enough
calibration only
Method 2 : enough
Method 1 : not enough
calibration only
Method 2 : enough
Variable : dependent on
the Position of the Orifice
Plunger
EnoughNot enough :
buffer zone
(two TMPs Required)
Not enough :
fixed orifice constraint
AnyMolecule, XEasy :
direct measurement
Easy :
direct measurement
DifficultIndefinite Traceability
QMS Dependent Signal
Indefinite Traceability,
QMS Dependent Signal
Modification
required
Atomic Mass200200200200200200
Uncerainty18.0%(BPG 400 IG)4.8% or 18.0%Conductance DependentUnknownUnknown4.8% (370 Stavil IG)
DAQ SoftwareReal TimeReal Time
(user specitied)
Not Real TimeReal TimeReal TimeReal Time
MaintenanceEasyEasyEasyVery DifficultVery DifficultEasy
CompetitivenessMost CompetitiveHighly CompetitiveCompetitiveHighly CompetitiveVery CompetitiveVery Competitive

(1) P.A.Redhead, “Recommended practices for measuring and reporting outgassing data”, J.Vac.Sci. Technol.A 20(5). Sep/Oct 2002
(2) US 5,528,032(June18,1996) - Thermal Desorption Gas Spectrometer, ESCO Ltd.